Application of radioisotope XRF for the determination of noble metals in aqueous solutions
Identifieur interne : 000955 ( Main/Exploration ); précédent : 000954; suivant : 000956Application of radioisotope XRF for the determination of noble metals in aqueous solutions
Auteurs : RBID : ISTEX:10967_1977_Article_BF02518013.pdfAbstract
Radiometric methods of determination of platium and palladium (0.1 to 5% of Pt and 0.1 to 2% of Pd), gold and indium (0.01 to 1% of Au and 1 to 4 g In/l) and of platinum and rhodium (0.1 to 9% of Pt and 0.05 to 1% of Rh) in aqueous solution has been worked out. A suitable measuring device has been designed and constructed. The methods are based on the measurement of characteristic radiation of the Lα line for gold and platinum and of the K-series for indium, palladium and rhodium, as well as on the measurement of scattered radiation from a238Pu source. The r.m.s. error of the determination varies from 0.01 to 0.10% of Pt, 0.002 to 0.01% of Au and 0.01 to 0.15% of Pd depending on the concentration. In the case of Rh and In the errors are 0.008% and 0.04 g In/l, respectively.
DOI: 10.1007/BF02518013
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Mickiewicza 30, 30-059, Cracow</wicri:regionArea><wicri:noRegion>Cracow</wicri:noRegion></affiliation></author><author><name>M. Lankosz</name><affiliation wicri:level="1"><mods:affiliation>Institute of Nuclear Physics and Techniques, University of Mining and Metallurgy, Al. Mickiewicza 30, 30-059, Cracow, (Poland)</mods:affiliation><country xml:lang="fr">Pologne</country><wicri:regionArea>Institute of Nuclear Physics and Techniques, University of Mining and Metallurgy, Al. Mickiewicza 30, 30-059, Cracow</wicri:regionArea><wicri:noRegion>Cracow</wicri:noRegion></affiliation></author><author><name>A. Markowicz</name><affiliation wicri:level="1"><mods:affiliation>Institute of Nuclear Physics and Techniques, University of Mining and Metallurgy, Al. Mickiewicza 30, 30-059, Cracow, (Poland)</mods:affiliation><country xml:lang="fr">Pologne</country><wicri:regionArea>Institute of Nuclear Physics and Techniques, University of Mining and Metallurgy, Al. Mickiewicza 30, 30-059, Cracow</wicri:regionArea><wicri:noRegion>Cracow</wicri:noRegion></affiliation></author><author><name>M. Wasilewska</name><affiliation wicri:level="1"><mods:affiliation>Institute of Nuclear Physics and Techniques, University of Mining and Metallurgy, Al. Mickiewicza 30, 30-059, Cracow, (Poland)</mods:affiliation><country xml:lang="fr">Pologne</country><wicri:regionArea>Institute of Nuclear Physics and Techniques, University of Mining and Metallurgy, Al. Mickiewicza 30, 30-059, Cracow</wicri:regionArea><wicri:noRegion>Cracow</wicri:noRegion></affiliation></author></titleStmt><publicationStmt><idno type="RBID">ISTEX:10967_1977_Article_BF02518013.pdf</idno><date when="1977">1977</date><idno type="doi">10.1007/BF02518013</idno><idno type="wicri:Area/Main/Corpus">000915</idno><idno type="wicri:Area/Main/Curation">000915</idno><idno type="wicri:Area/Main/Exploration">000955</idno></publicationStmt></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="eng">Radiometric methods of determination of platium and palladium (0.1 to 5% of Pt and 0.1 to 2% of Pd), gold and indium (0.01 to 1% of Au and 1 to 4 g In/l) and of platinum and rhodium (0.1 to 9% of Pt and 0.05 to 1% of Rh) in aqueous solution has been worked out. A suitable measuring device has been designed and constructed. The methods are based on the measurement of characteristic radiation of the Lα line for gold and platinum and of the K-series for indium, palladium and rhodium, as well as on the measurement of scattered radiation from a238Pu source. The r.m.s. error of the determination varies from 0.01 to 0.10% of Pt, 0.002 to 0.01% of Au and 0.01 to 0.15% of Pd depending on the concentration. In the case of Rh and In the errors are 0.008% and 0.04 g In/l, respectively.</div></front></TEI><mods xsi:schemaLocation="http://www.loc.gov/mods/v3 file:///applis/istex/home/loadistex/home/etc/xsd/mods.xsd" version="3.4" istexId="a00cf78bf919db2d7e24a494c3b5d2bf1d257f19"><titleInfo lang="eng"><title>Application of radioisotope XRF for the determination of noble metals in aqueous solutions</title></titleInfo><name type="personal"><namePart type="given">B.</namePart><namePart type="family">Hołyńska</namePart><role><roleTerm type="text">author</roleTerm></role><affiliation>Institute of Nuclear Physics and Techniques, University of Mining and Metallurgy, Al. Mickiewicza 30, 30-059, Cracow, (Poland)</affiliation></name><name type="personal"><namePart type="given">S.</namePart><namePart type="family">Kalita</namePart><role><roleTerm type="text">author</roleTerm></role><affiliation>Institute of Nuclear Physics and Techniques, University of Mining and Metallurgy, Al. Mickiewicza 30, 30-059, Cracow, (Poland)</affiliation></name><name type="personal"><namePart type="given">M.</namePart><namePart type="family">Lankosz</namePart><role><roleTerm type="text">author</roleTerm></role><affiliation>Institute of Nuclear Physics and Techniques, University of Mining and Metallurgy, Al. Mickiewicza 30, 30-059, Cracow, (Poland)</affiliation></name><name type="personal"><namePart type="given">A.</namePart><namePart type="family">Markowicz</namePart><role><roleTerm type="text">author</roleTerm></role><affiliation>Institute of Nuclear Physics and Techniques, University of Mining and Metallurgy, Al. Mickiewicza 30, 30-059, Cracow, (Poland)</affiliation></name><name type="personal"><namePart type="given">M.</namePart><namePart type="family">Wasilewska</namePart><role><roleTerm type="text">author</roleTerm></role><affiliation>Institute of Nuclear Physics and Techniques, University of Mining and Metallurgy, Al. Mickiewicza 30, 30-059, Cracow, (Poland)</affiliation></name><typeOfResource>text</typeOfResource><genre>Physical Methods Section</genre><genre>Original Paper</genre><originInfo><publisher>Kluwer Academic Publishers, Dordrecht</publisher><dateCreated encoding="w3cdtf">1976-04-01</dateCreated><dateValid encoding="w3cdtf">2006-10-07</dateValid><copyrightDate encoding="w3cdtf">1977</copyrightDate></originInfo><language><languageTerm type="code" authority="iso639-2b">eng</languageTerm></language><physicalDescription><internetMediaType>text/html</internetMediaType></physicalDescription><abstract lang="eng">Radiometric methods of determination of platium and palladium (0.1 to 5% of Pt and 0.1 to 2% of Pd), gold and indium (0.01 to 1% of Au and 1 to 4 g In/l) and of platinum and rhodium (0.1 to 9% of Pt and 0.05 to 1% of Rh) in aqueous solution has been worked out. A suitable measuring device has been designed and constructed. The methods are based on the measurement of characteristic radiation of the Lα line for gold and platinum and of the K-series for indium, palladium and rhodium, as well as on the measurement of scattered radiation from a238Pu source. The r.m.s. error of the determination varies from 0.01 to 0.10% of Pt, 0.002 to 0.01% of Au and 0.01 to 0.15% of Pd depending on the concentration. In the case of Rh and In the errors are 0.008% and 0.04 g In/l, respectively.</abstract><relatedItem type="series"><titleInfo type="abbreviated"><title>J. Radioanal. Chem.</title></titleInfo><titleInfo><title>Journal of Radioanalytical Chemistry</title><subTitle>International Journal dealing with all aspects of nuclear analytical methods</subTitle><partNumber>Year: 1977</partNumber><partNumber>Volume: 35</partNumber><partNumber>Number: 2</partNumber></titleInfo><genre>Archive Journal</genre><originInfo><dateIssued encoding="w3cdtf">1977-09-01</dateIssued><copyrightDate encoding="w3cdtf">1977</copyrightDate></originInfo><subject usage="primary"><topic>Chemistry</topic><topic>Inorganic Chemistry</topic><topic>Physical Chemistry</topic><topic>Nuclear Chemistry</topic><topic>Diagnostic Radiology</topic><topic>Nuclear Physics, Heavy Ions, Hadrons</topic></subject><identifier type="issn">0022-4081</identifier><identifier type="issn">Electronic: 1588-2780</identifier><identifier type="matrixNumber">10967</identifier><identifier type="local">IssueArticleCount: 18</identifier><recordInfo><recordOrigin>Akadémiai Kiadó, 1977</recordOrigin></recordInfo></relatedItem><identifier type="doi">10.1007/BF02518013</identifier><identifier type="matrixNumber">Art13</identifier><identifier type="local">BF02518013</identifier><accessCondition type="use and reproduction">MetadataGrant: OpenAccess</accessCondition><accessCondition type="use and reproduction">AbstractGrant: OpenAccess</accessCondition><accessCondition type="restriction on access">BodyPDFGrant: Restricted</accessCondition><accessCondition type="restriction on access">BodyHTMLGrant: Restricted</accessCondition><accessCondition type="restriction on access">BibliographyGrant: Restricted</accessCondition><accessCondition type="restriction on access">ESMGrant: Restricted</accessCondition><part><extent unit="pages"><start>361</start><end>371</end></extent></part><recordInfo><recordOrigin>Akadémiai Kiadó, 1977</recordOrigin><recordIdentifier>10967_1977_Article_BF02518013.pdf</recordIdentifier></recordInfo></mods></record>Pour manipuler ce document sous Unix (Dilib)
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